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He hasn't, but his icy air is cold enough to prevent someone from breathing and can destroy their cells in an extremely short period of time, which I don't think is comparable to freezing air itself so it might not be relevantDid Douma freeze air itself ever? We can get a temperature very easily from all of those feats you just listed but the air freezing is probably the only relevant end tbh.
Freezing air requires some low ass temperatures.